HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentanone → Methyl2-[(cyclopentylamino)methyl]-2-ethyl-butanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentanone | HCID 8452 | — |
| Reactant | Methyl2-ethyl-2-[(propan-2-ylamino)methyl]butanoate | HCID 86617586 | — |
| Product | Methyl2-[(cyclopentylamino)methyl]-2-ethyl-butanoate | HCID 68684960 | — |
Reaction Steps
The title compound was prepared by an analogous method to the preparation of Intermediate 200, on a 50 mmol scale utilising Cyclopentanone (Aldrich; 6.33 g, 75 mmol), and distillation at 50° C. and 0.53 mbar pressure, as a clear oil (7.5 g, 65%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07709471B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-8e6f5bfec7c5450e8aa0a3bf0972a4fd |
| Source note | uspto-grants-2010_05 |