HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21920917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Fluorobenzoyl chloride | HCID 67879 | — |
| Reactant | 4-Methyl-2,3-dihydro-1H-inden-2-amine | HCID 12337208 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 21920917 | HCID 21920917 | — |
Reaction Steps
370 mg (2.52 mmol) 2-amino-4-methylindane and 257 mg (2.52 mmol) triethylamine were dissolved in 5 ml dioxane, 400 mg (2.52 mmol) 4-fluorobenzoylchloride were added, and the mixture was stirred for 2 h at room temperature (RT).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713963B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-9c91932c5f2e45f196fcb05d1a288e99 |
| Source note | uspto-grants-2010_05 |