HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl formate → HCID 11659015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | HCID 11447790 | HCID 11447790 | — |
| Product | HCID 11659015 | HCID 11659015 | — |
Reaction Steps
To 10 ml of ethyl format was added 0.4 g of 3-(5-Chloro-pyridin-2-yloxy)-8-aza-bicyclo[3.2.1]octane, the mixture was heated at reflux for 48 hours and evaporated to dryness, crystallized from ethyl acetate petroleum ether. Yield 200 mg (53%), Mp. 112-114° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713990B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-bd980439e6e74067a6b0b7bd2da523e6 |
| Source note | uspto-grants-2010_05 |