HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dimethyl-2-(2-phenoxyacetamido)ethylamine → Hydrochloric Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dimethyl-2-(2-phenoxyacetamido)ethylamine | HCID 11806274 | — |
| Reactant | 4-Amino-3,5-dichlorophenylglyoxal hydrate | HCID 20521529 | — |
| Product | Hydrochloric Acid | HCID 313 | — |
| Product | 1-(4-Amino-3,5-dichlorophenyl)-2-[1,1-dimethyl-2-(2-phenoxyacetamido)ethylamino]ethanol | HCID 54086741 | — |
Reaction Steps
In a similar manner but using 1,1-dimethyl-2-(2-phenoxyacetamido)ethylamine and 4-amino-3,5-dichlorophenylglyoxal hydrate as starting materials there was obtained 1-(4-amino-3,5-dichlorophenyl)-2-[1,1-dimethyl-2-(2-phenoxyacetamido)ethylamino]ethanol (Example 2) in 35% yield, m.p. 107°-9° C. (hydrochloride, monohydrate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04355045 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-0d2c274e2e0d46bcac9c31c8b7e52d6f |
| Source note | uspto-grants-1982_10 |