HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68690173, compound → HCID 68688989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68690173 | HCID 68690173 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68688989 | HCID 68688989 | — |
Reaction Steps
To a solution of the compound prepared in Example 46 (4.77 g) in ethanol (140 mL) was added 5% palladium/carbon (0.5 g) and the mixture was stirred at room temperature for 2 hours under an atmosphere of hydrogen. The reaction mixture was filtrated with Celite (proprietary name) and the filtrate was concentrated to give the compound of the present invention (2.93 g) having the following physical data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713998B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-d33b55751d54445f82b40056ea86a859 |
| Source note | uspto-grants-2010_05 |