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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2235045Generated: November 1, 2026

HCID 68690173, compound → HCID 68688989, compound

https://huagongshe.com/reaction/2235045

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68690173HCID 68690173—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 68688989HCID 68688989—

Reaction Steps

To a solution of the compound prepared in Example 46 (4.77 g) in ethanol (140 mL) was added 5% palladium/carbon (0.5 g) and the mixture was stirred at room temperature for 2 hours under an atmosphere of hydrogen. The reaction mixture was filtrated with Celite (proprietary name) and the filtrate was concentrated to give the compound of the present invention (2.93 g) having the following physical data.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07713998B2
Source datasetuspto-grants-2010_05
ORD IDord-d33b55751d54445f82b40056ea86a859
Source noteuspto-grants-2010_05