HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131728112, compound → HCID 67526328, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131728112 | HCID 131728112 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67526328 | HCID 67526328 | — |
Reaction Steps
45 mg (98 μmol) benzyl(R)-{1-[3-methyl-4-(pyrrolidine-1-sulphonyl)-phenyl]-5-oxo-pyrrolidin-3-yl}-carbamate are dissolved in 10 ml of methanol, combined with 25 mg palladium on charcoal and hydrogenated for 8 hours in a Parr apparatus at 3 bar hydrogen pressure at ambient temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714000B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-c46d1e9a97c64696aced9c4089522a2b |
| Source note | uspto-grants-2010_05 |