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HRID2235170

反应详情

EQUATION

反应方程式

HRID 2235170 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(Cl)cc1S(=O)(=O)Cl
HCID2734272

5-chloro-2-methoxybenzenesulfonyl chloride

C7H6Cl2O3S

结构：Brc1ccc2c(c1)NCCCC2
HCID16244474

8-Bromo-2,3,4,5-tetrahydro-1H-1-benzazepine

C10H12BrN

PRODUCTS

生成物

1
结构：COc1ccc(Cl)cc1S(=O)(=O)N1CCCCc2ccc(Br)cc21
HCID68435027

未命名化合物

PROCEDURE

实验过程

8-Bromo-2,3,4,5-tetrahydro-1H-benzo[b]azepine was reacted with 5-chloro-2-methoxybenzenesulfonyl chloride in analogy to example 34, step 2, yielding 8-bromo-1-(5-chloro-2-methoxy-benzenesulfonyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepine. Off-white solid, MS (ISP): m/e 430.2 (M+H).