HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methoxybenzene-1-sulfonyl chloride → 8-bromo-1-(5-chloro-2-methoxy-benzenesulfonyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methoxybenzene-1-sulfonyl chloride | HCID 2734272 | — |
| Reactant | 8-Bromo-2,3,4,5-tetrahydro-1H-benzo[b]azepine | HCID 16244474 | — |
| Product | 8-bromo-1-(5-chloro-2-methoxy-benzenesulfonyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepine | HCID 68435027 | — |
Reaction Steps
8-Bromo-2,3,4,5-tetrahydro-1H-benzo[b]azepine was reacted with 5-chloro-2-methoxybenzenesulfonyl chloride in analogy to example 34, step 2, yielding 8-bromo-1-(5-chloro-2-methoxy-benzenesulfonyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepine. Off-white solid, MS (ISP): m/e 430.2 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713996B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-56b7a819f4214434928af3029f74f11e |
| Source note | uspto-grants-2010_05 |