HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 59299343, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 59299455 | HCID 59299455 | — |
| Product | HCID 59299343 | HCID 59299343 | 61% |
Reaction Steps
Prepare essentially as described in Example 228, using 3-(4-bromo-2-chloro-benzyl)-1-cyclohexyl-piperidin-2-one and aniline. Evaporate the crude reaction mixture and purify by chromatography on silica gel to give the title compound (127 mg, 61%). MS (ES+) m/z=383 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713979B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-372d106c75574e53ab7150dc64fcdefb |
| Source note | uspto-grants-2010_05 |