HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2235319Generated: October 31, 2026
Hydrochloric Acid → HCID 178479619, compound
https://huagongshe.com/reaction/2235319
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178455340 | HCID 178455340 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178479619 | HCID 178479619 | 147.4% |
Reaction Steps
Add HCl (0.015 mL) to 1-[cis-4-(tert-butyl-dimethyl-silanyloxy)-cyclohexyl]-3-(2,6-dichloro-4-pyridin-3-yl-benzyl)-pyrrolidin-2-one (Preparation 75) (0.027 G, 0.0506 mmol) in methanol (2 mL) and heat to 40° C. for 1 hour. Concentrate under reduced pressure to give the title compound (0.017 g): mass spectrum (m/z):420(M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07713979B2 |
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| Source dataset | uspto-grants-2010_05 |
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| ORD ID | ord-7aa50012cc1b4622afb0ab9d78b7c9f9 |
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| Source note | uspto-grants-2010_05 |
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