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HRID2235404

反应详情

EQUATION

反应方程式

HRID 2235404 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)/C=C/c1ccccc1[N+](=O)[O-]
HCID12561348

(2E)-3-(2-Nitrophenyl)-2-propenoyl chloride

C9H6ClNO3

结构：CCCCCN1C(=O)C(C)(C)c2cc(N)c([N+](=O)[O-])cc21
HCID17802744

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCN1C(=O)C(C)(C)c2cc(NC(=O)/C=C/c3ccccc3[N+](=O)[O-])c([N+](=O)[O-])cc21
HCID23092686

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

To a solution of A8 (0.6 g) is added freshly prepared (E)-3-(2-nitro-phenyl)-acryloyl chloride (0.7 g; 3,31 mmol). The mixture is stirred for 2 h at RT in dry CH2Cl2 (15 ml). After an aqueous work-up the compound is obtained as a yellow solid.

WORKUP

后处理

  1. customAfter an aqueous work-up the compound is obtained as a yellow solid