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HRID2235414

反应详情

EQUATION

反应方程式

HRID 2235414 的结构方程式

REACTANTS

反应物

1
结构：CCCCCN1C(=O)C(C)(C)c2cc(N(C)C(=O)CCc3ccccc3)c([N+](=O)[O-])cc21
HCID23092651

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCN1C(=O)C(C)(C)c2cc3c(cc21)nc(CCc1ccccc1)n3C
HCID59300923

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO.ClCCl
溶剂HCID21226129

未命名化合物

PROCEDURE

实验过程

1,7,7-Trimethyl-5-pentyl-2-phenethyl-5,7-dihydro-1H-imidazo[4,5-f]indol-6-one is prepared from crude N-(3,3-dimethyl-6-nitro-2-oxo-1-pentyl-2,3-dihydro-1H-indol-5-yl)-N-methyl-3-phenyl-propionamide as described in Example 3b. The desired compound (78 mg) is obtained by flash chromatography on silica gel eluting with CH2Cl2/MeOH (98:2).