HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 59300846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 4-Phenylbutanoyl Chloride | HCID 11789865 | — |
| Reactant | 5-Amino-3,3-dimethyl-6-nitro-1-pentyl-1,3-dihydro-indol-2-one | HCID 17802744 | — |
| Product | HCID 59300846 | HCID 59300846 | 12.6% |
Reaction Steps
1-Ethyl-7,7-dimethyl-5-pentyl-2-(3-phenyl-propyl)-5,7-dihydro-1H-imidazo[4,5-f]indol-6-one (36 mg) is synthesized from A8 (200 mg), freshly prepared 4-phenyl-butyryl chloride (150 mg; 0.82 mmol) and ethyl iodide (70 μl; 0.87 mmol) as described in Example 57.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714010B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-06e02ba3d80440348347200b14d986fc |
| Source note | uspto-grants-2010_05 |