HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23092668, compound → HCID 17802736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23092668 | HCID 23092668 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 17802736 | HCID 17802736 | — |
Reaction Steps
The crude N-methyl-N-(1,3,3-trimethyl-6-nitro-2-oxo-2,3-dihydro-1H-indol-5-yl)-acetamide is dissolved in hydrochloric acid (6 N; 8 ml) and heated at reflux for 3 h. The mixture is poured into ice-water and the resulting precipitate collected by filtration. After drying the compound (176 mg) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714010B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-7605ede9eaab4354a8aab33f818ccb7c |
| Source note | uspto-grants-2010_05 |