HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23092672, compound → HCID 59300794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23092672 | HCID 23092672 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 59300794 | HCID 59300794 | 91.5% |
Reaction Steps
A solution of (E)-3-phenyl-N-(1,3,3-trimethyl-6-methylamino-2-oxo-2,3-dihydro-1H-indol-5-yl)-acrylamide (288 mg) in acetic acid (6 ml) is heated under reflux for 1 h. After recooling the mixture is poured into ice-water whereupon the desired compound (250 mg) is precipitated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714010B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-2485e187091249edb8996026afb40c92 |
| Source note | uspto-grants-2010_05 |