Hydrochloric Acid → HCID 59301006, compound

Participants

Reaction Steps

[(S)-1-(7,7-Dimethyl-6-oxo-5-pentyl-1,5,6,7-tetrahydro-imidazo[4,5-f]indol-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester (50 mg) is treated with a mixture of 1,4-dioxane (5 ml) and hydrochloric acid (2 N; 5 ml) for 15 min at 50° C. The solvents are evaporated and the residue lyophilized. The desired compound (43 mg) is obtained as a hydrochloride (white solid).

Provenance & Evidence