HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67427131, compound → 1H-Imidazole-2-propanoic acid, 1-methyl-, methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67427131 | HCID 67427131 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1H-Imidazole-2-propanoic acid, 1-methyl-, methyl ester | HCID 67426926 | — |
Reaction Steps
(E)-3-(1-Methyl-1H-imidazol-2-yl)-acrylic acid methyl ester (0.86 g) is dissolved in MeOH (10 ml) and hydrogenated at 3 bar at RT for 2 h using Pd/C (10%, 0.1 g) as catalyst. After filtration and evaporation of the solvent the compound (0.87 g) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714010B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-a35faaa769714fa3b1d6fbd0beced650 |
| Source note | uspto-grants-2010_05 |