Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 59300970 | HCID 59300970 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 67426354 | HCID 67426354 | — |
Reaction Steps
E1 (330 mg) is dissolved in CHCl3 (5 ml), thionyl chloride (1.2 ml) is added and the mixture is stirred at 60° C. for 15 h. The reaction mixture is concentrated in vacuo to give the compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07714010B2 |
|---|
| Source dataset | uspto-grants-2010_05 |
|---|
| ORD ID | ord-c882e97962164686bf276b409c0e46c9 |
|---|
| Source note | uspto-grants-2010_05 |
|---|
