Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 59300882 | HCID 59300882 | — |
| Product | HCID 59300953 | HCID 59300953 | 10.6% |
Reaction Steps
A mixture of F1 (100 mg) and benzylamine (1.5 ml; 13.6 mmol) is stirred in a microwave apparatus at 200° C. for 8 min. After re-cooling the mixture is concentrated in vacuo and purified by RP-MPLC (Polygoprep 100-50 C18) eluting with a water/MeCN gradient to give the desired compound (13 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07714010B2 |
|---|
| Source dataset | uspto-grants-2010_05 |
|---|
| ORD ID | ord-0c994dc7f2d94fb1b47eda75ddb13c09 |
|---|
| Source note | uspto-grants-2010_05 |
|---|
