L-Tartaric acid → HCID 86595686, compound

HRID 2235834Notes

Reaction equation

HRID 2235834 reaction equation
[CH3:1][NH:2][CH2:3][CH2:4][CH2:5][C@:6]1([C:17]2[CH:18]=[CH:19][C:20]([F:23])=[CH:21][CH:22]=2)[O:14][CH2:13][C:12]2[CH:11]=[C:10]([C:15]#[N:16])[CH:9]=[CH:8][C:7]1=2.[C:24]([OH:33])(=[O:32])[C@@H:25]([C@H:27]([C:29]([OH:31])=[O:30])[OH:28])[OH:26]>CO.O>[CH3:1][NH:2][CH2:3][CH2:4][CH2:5][C@:6]1([C:17]2[CH:18]=[CH:19][C:20]([F:23])=[CH:21][CH:22]=2)[O:14][CH2:13][C:12]2[CH:11]=[C:10]([C:15]#[N:16])[CH:9]=[CH:8][C:7]1=2.[C:29]([C@@H:27]([C@H:25]([C:24]([O-:33])=[O:32])[OH:26])[OH:28])([O-:31])=[O:30]

Participants

5

Reactant 2

HCID 444305L-Tartaric acidHCID 12986614HCID 12986614, compound

Product 1

HCID 86595686HCID 86595686, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Procedure

To a desmethylcitalopram (1.2 g) solution in Methanol (15 ML) was added a solution of L-tartaric acid (0.58 g) in water (2 mL). The reaction mixture was stirred at room temperature for 1 h.

Sources & evidence

ORD record
ord-c0471ca4cbdf46ffb82d2c30a6f3ad51
Source dataset
uspto-grants-2010_05
Patent number
US07714023B2

Reaction notes

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