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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2235996Generated: November 1, 2026

HCID 59853915, compound → HCID 59853913, compound

https://huagongshe.com/reaction/2235996

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59853915HCID 59853915—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
SolventHCID 178418361HCID 178418361—
ProductHCID 59853913HCID 59853913—

Reaction Steps

100 mg of palladium carbon (10% w/v) was added to 105 mg (0.261 mmol) of ethyl 2-[4-(5H-dibenzo[a,d][7]annulen-5-ylidene)-1-piperidinyl]-2-oxoethylcarbamate in 3 ml of ethanol, and they were stirred at 3.6 MPa in hydrogen gas atmosphere overnight. After the filtration, the solvent was evaporated under reduced pressure to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07713957B2
Source datasetuspto-grants-2010_05
ORD IDord-98bc663c998e47b2b99877d35f383e54
Source noteuspto-grants-2010_05