HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59853915, compound → HCID 59853913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59853915 | HCID 59853915 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | HCID 59853913 | HCID 59853913 | — |
Reaction Steps
100 mg of palladium carbon (10% w/v) was added to 105 mg (0.261 mmol) of ethyl 2-[4-(5H-dibenzo[a,d][7]annulen-5-ylidene)-1-piperidinyl]-2-oxoethylcarbamate in 3 ml of ethanol, and they were stirred at 3.6 MPa in hydrogen gas atmosphere overnight. After the filtration, the solvent was evaporated under reduced pressure to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713957B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-98bc663c998e47b2b99877d35f383e54 |
| Source note | uspto-grants-2010_05 |