Benzoyl chloride → HCID 11646668, compound

HRID 2236075Notes

Reaction equation

HRID 2236075 reaction equation
[CH3:1][C:2]([O:5][C:6]([N:8]1[CH2:13][CH2:12][C:11]2[C:14]([C:18]#[N:19])=[C:15]([NH2:17])[S:16][C:10]=2[CH2:9]1)=[O:7])([CH3:4])[CH3:3].[C:20](Cl)(=[O:27])[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[C:2]([O:5][C:6]([N:8]1[CH2:13][CH2:12][C:11]2[C:14]([C:18]#[N:19])=[C:15]([NH:17][C:20](=[O:27])[C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)[S:16][C:10]=2[CH2:9]1)=[O:7])([CH3:1])([CH3:3])[CH3:4]

Participants

3

Reactant 2

HCID 7412Benzoyl chlorideHCID 2763861tert-butyl 2-amino-3-cyano-4,7-dihydrothieno[2,3-c]pyridine-6(5H)-carboxylate2×

Product 1

HCID 11646668HCID 11646668, compound

Procedure

Prepared according to general procedure A starting from 2-amino-3-cyano-4,7-dihydro-thieno[2,3-c]pyridine-6(5H)-carboxylic acid 1,1-dimethylethyl ester (compound A2) and benzoyl chloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-95bbd5edc57b46cca197e50bf9f3dd43
Source dataset
uspto-grants-2010_05
Patent number
US07714134B2

Reaction notes

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