HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 43430863, compound → HCID 86616318, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 43430863 | HCID 43430863 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 86616318 | HCID 86616318 | — |
Reaction Steps
100 mg of N-(3-cyano4,5,6,7-tetrahydro-thieno[2,3-c]pyridin-2-yl)-benzamide (compound B2) and 57 mg of ethylchlorothioformiate are dissolved in 2 ml of pyridine. After stirring for 3 hours at room temperature, the solvent is removed and the remaining residue recristallized from ethanol to obtain the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714134B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-564597229a7941d9af9f0df9b0904983 |
| Source note | uspto-grants-2010_05 |