Phenylhydrazine → Ethyl (6-chloro-1,2,3,4-tetrahydro-pyrido[4,3-b]indol-5-yl)-acetate hydrochloride

HRID 2236100Notes

Reaction equation

HRID 2236100 reaction equation
[ClH:1].[CH2:2]1[C:14]2[C:13]3[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=3[N:7]([CH2:15][C:16]([O:18][CH2:19][CH3:20])=[O:17])[C:6]=2[CH2:5][CH2:4][NH:3]1.C1(NN)C=CC=CC=1>>[ClH:1].[Cl:1][C:9]1[C:8]2[N:7]([CH2:15][C:16]([O:18][CH2:19][CH3:20])=[O:17])[C:6]3[CH2:5][CH2:4][NH:3][CH2:2][C:14]=3[C:13]=2[CH:12]=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 71552668Ethyl (1,2,3,4-tetrahydro-pyrido[4,3-b]indol-5-yl)-acetate hydrochloride

Product 1

HCID 86614335Ethyl (6-chloro-1,2,3,4-tetrahydro-pyrido[4,3-b]indol-5-yl)-acetate hydrochloride

Procedure

The title compound is prepared using a procedure analogous to Intermediate 1, substituting 2-chlorophenylhydrazine for phenylhydrazine in Step 1a).

Sources & evidence

ORD record
ord-56beb04babb94414b1be26f670370e7e
Source dataset
uspto-grants-2010_05
Patent number
US07714132B2

Reaction notes

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