HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 25264202, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Oxindole | HCID 321710 | — |
| Reactant | HCID 86620348 | HCID 86620348 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 25264202 | HCID 25264202 | — |
Reaction Steps
20 mg (4Z,6Z,8E)-2-(dimethylamino)cyclohepta[b]pyrrole-3-carbaldehyde, 25 mg oxindole, and 0.1 mg piperidine were added in IPA with reflux for 20 hours. After cooling, red crystals were precipitated. After filtration and washing by IPA, Compound 035 was obtained (55%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714146B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-aebbc2d55674442bafda6e0a9a6aa9c3 |
| Source note | uspto-grants-2010_05 |