Ammonium Hydroxide → HCID 178512964, compound

HRID 2236136Notes

Reaction equation

HRID 2236136 reaction equation
[NH2:1][C@H:2]([C:10]([OH:12])=[O:11])[CH2:3][CH2:4][CH2:5][NH:6][C:7](=[NH:9])[NH2:8].[OH-].[NH4+:14]>O>[NH2:1][CH:2]([CH2:3][CH2:4][CH2:5][NH:6][C:7]([NH2:9])=[NH:8])[C:10]([O-:12])=[O:11].[NH4+:14]

Participants

4

Reactant 2

HCID 14923Ammonium HydroxideHCID 178418600HCID 178418600, compound

Product 1

HCID 178512964HCID 178512964, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Separately, in a single-necked, round bottomed flask, equipped with a magnetic stirrer, 10.45 g (60 mmol) of Arginine is dissolved in 300 ml of water. To this is added 78 ml of 1M ammonium hydroxide with vigorous stirring, until heat production ceases. At this point the water is removed by evaporation to yield the carboxylate salt, ammonium 2-amino-5-guanidinopentanoate, shown below.

Workup

  1. customSeparately, in a single-necked, round bottomed flask, equipped with a magnetic stirrer
  2. temperatureuntil heat production ceases
  3. customAt this point the water is removed by evaporation

Sources & evidence

ORD record
ord-4d08f9a8a3474efe9f15d3eadbe7e6b7
Source dataset
uspto-grants-2010_05
Patent number
US07714154B2

Reaction notes

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