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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2236161Generated: October 30, 2026

HCID 67536157, compound → HCID 59301332, compound

https://huagongshe.com/reaction/2236161

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67536157HCID 67536157—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 59301332HCID 59301332—

Reaction Steps

This nitro compound was dissolved in 10 mL of EtOAc, and treated with 100 mg of 10% palladium on carbon. The reaction was shaken under 50 psi of H2 overnight. The reaction was filtered through a celite pad, and the filtrate was concentrated to afford 6-(3-methoxy-pyrrolidin-1-yl)-pyridin-3-ylamine, which was used directly in the next step without further purification. LRMS calcd for C10H15N3O (m/e) 193, obsd 194 (M+H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07714126B2
Source datasetuspto-grants-2010_05
ORD IDord-a728d5dad97f4ca08f6bf5bba1ef9991
Source noteuspto-grants-2010_05