HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-nitropyridine → HCID 67536866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-nitropyridine | HCID 78308 | — |
| Reactant | Methoxyisopropylamine | HCID 123458 | — |
| Product | HCID 67536866 | HCID 67536866 | — |
Reaction Steps
This compound was prepared with the same method described before by using 2-methoxy-1-methylethylamine and 2-chloro-5-nitro-pyridine to give N-(2-methoxy-1-methylethyl)-2-amino-5-nitro-pyridine. LCMS calcd for C9H13N3O3 m/e 211.22, obsd 210.2 (AP, M−H). The nitro compound was hydrogenated under the same condition described before to give N2-(2-methoxy-1-methylethyl)-2,5-diaminopyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714126B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-b9ccc7ba0cc84b75b65640107d55d964 |
| Source note | uspto-grants-2010_05 |