HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-methyl-2-phenyl-2H-1,2,3-triazole-4-carboxylic acid → 5-methyl-2-phenyl-2H-[1,2,3]triazole-4-carboxylic acid {6-[methyl-(2,2,2-trifluoro-ethyl)-amino]-pyridin-3-yl}-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-methyl-2-phenyl-2H-1,2,3-triazole-4-carboxylic acid | HCID 519936 | — |
| Reactant | 2,5-Pyridinediamine, N2-methyl-N2-(2,2,2-trifluoroethyl)- | HCID 59301305 | — |
| Product | 5-methyl-2-phenyl-2H-[1,2,3]triazole-4-carboxylic acid {6-[methyl-(2,2,2-trifluoro-ethyl)-amino]-pyridin-3-yl}-amide | HCID 59301427 | — |
Reaction Steps
With a procedure similar to example 16 above, 5-methyl-2-phenyl-2H-[1,2,3]triazole-4-carboxylic acid {6-[methyl-(2,2,2-trifluoro-ethyl)-amino]-pyridin-3-yl}-amide was prepared from 5-methyl-2-phenyl-2H-[1,2,3]triazole-4-carboxylic acid and N2-methyl-N2-(2,2,2-trifluoro-ethyl)-pyridine-2,5-diamine. LCMS calcd for C18H17F3N6O (m/e) 390, obsd 391 (M+H). The NMR spectrum obtained on the sample is compatible with its structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07714126B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-a75d91733996439396ae63b2aa6025d9 |
| Source note | uspto-grants-2010_05 |