HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 73678927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Hydroxylamine, sulfate (1:1) | HCID 159255 | — |
| Reactant | HCID 20436102 | HCID 20436102 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 73678927 | HCID 73678927 | 191% |
Reaction Steps
The procedure described in Example 1(b) is repeated, except that 223 g (1 mol) of 3,3-dimethyl-12-ethyl-1-aza-cyclododecene, 82 g (0.5 mol) of hydroxylamine sulfate, 150 g of sulfuric acid and 400 ml of water are used. Distillation yields 245 g (0.955 mol) of 2,2-dimethyl-11-ethyl-11-amino-undecanal oxime; yield 95.5% of theory; boiling point 155°-160° C./7 Pa.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04355177 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-003a1ecf84da407da9380d654df73c97 |
| Source note | uspto-grants-1982_10 |