2-(Tributylstannyl)furan → HCID 42625595, compound

Participants

Reaction Conditions

Reaction Steps

3-Hydroxy-4-iodo-benzonitrile (120 mg, 0.49 mmol) and PdCl2(PPh3)2 (35 mg, 0.049 mmol) and 2-furyltributyltin (200 g, 0.56 mmol) in N,N-dimethylformamide (DMF) (5 mL) is degassed and heated at 100° C. for 30 minutes (min). After the mixture cooled to room temperature, an aqueous work up is performed and the product is isolated from chromatography (80 mg, 88%).

Provenance & Evidence