HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2,2-Dimethyl-11-isopropyl-11-amino-undecanal benzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3,3-Dimethyl-12-isopropyl-1-aza-cyclododecene | HCID 20436097 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2,2-Dimethyl-11-isopropyl-11-amino-undecanal benzylamine | HCID 86737849 | 56.4% |
Reaction Steps
The procedure described in Example 2(b) is repeated, except that 68.5 g (0.5 mol) of 3,3-dimethyl-12-isopropyl-1-aza-cyclododecene, 50 g of 37% hydrochloric acid, 54 g (0.5 mol) of benzylamine and 200 ml of water are used. After neutralisation with 22 g (0.55 mol) of solid sodium hydroxide, 97 g (0.282 mol) of 2,2-dimethyl-11-isopropyl-11-amino-undecanal-benzylamine are obtained; yield 56.4% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04355177 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-ee0f14f94709454c85f67d1eab9649d0 |
| Source note | uspto-grants-1982_10 |