HRID2236512

反应详情

EQUATION

反应方程式

HRID 2236512 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

[1-(2-Fluoro-4-nitro-phenyl)-pyrrolidin-2-ylmethyl]-dimethyl-amine (77 mg, 0.29 mmol) and Pd/C (16 mg, 10% weight) is shaken under H2 (50 psi) in MeOH overnight. After filtrating the Pd/C, the MeOH is removed and the residue obtained (65 mg, 95%) is directly employed in the next step.

WORKUP

后处理

  1. filtrationAfter filtrating the Pd/C
  2. customthe MeOH is removed
  3. customthe residue obtained (65 mg, 95%)