1H-Indazol-6-amine → HCID 178518310, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 4-methoxymethylene-4H-isoquinoline-1,3-dione (101.5 mg, 0.5 mmol), 1H-indazol-6-ylamine (66.6 mg, 0.5 mmol) in 1 mL of N,N-dimethylformamide is heated at 110° C. for 1 h. After cooling in the refrigerator, the precipitate is collected, and washed with ether to give 79.4 mg (52%) of yellow solid mp >300° C.; MS (ESI) m/z 305.10 (M+1);

Provenance & Evidence