HRID2236598

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID846150

4-(piperidin-1-ylmethyl)aniline

C12H18N2

结构：CO/C=C1/C(=O)NC(=O)c2ccc([N+](=O)[O-])cc21

HCID59300161

未命名化合物

$结构：Cn1ccnc1Sc1ccc(N/C=C2\C(=O)NC(=O)c3ccccc32)cc1Cl$

HCID178480603

未命名化合物

PRODUCTS

生成物

结构：O=C1NC(=O)c2ccc([N+](=O)[O-])cc2/C1=C/Nc1ccc(CN2CCCCC2)cc1

HCID178518386

未命名化合物

收率 73.3%

PROCEDURE

实验过程

Using the procedure described for (4Z)-4-[({3-chloro-4-[(1-methyl-1H-imidazol-2-yl)thio]phenyl}amino)methylene]isoquinoline-1,3(2H,4H)-dione, 115 mg (0.46 mmol) of (4E)-4-(methoxy)methylene-6-nitroisoquinoline-1,3(2H,4H)-dione is reacted with 93 mg (0.49 mmol) of 4-piperidin-1-ylmethyl-phenylamine to give 137 mg (73%) of brown solid, mp 225-235 (dec); MS (ES−) m/z 405.2 (M−H)−1.