HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59300285, compound → HCID 178440917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59300285 | HCID 59300285 | — |
| Reactant | 4-methoxymethylene-6-iodo-4H-isoquinoline-1,3-dione | HCID 68691019 | — |
| Reactant | HCID 178518360 | HCID 178518360 | — |
| Product | HCID 178440917 | HCID 178440917 | 65% |
Reaction Steps
Following the same procedure for the preparation of 4-{[(2-Hydroxy-biphenyl-4-ylmethyl)-amino]-methylene}-6-iodo-4H-isoquinoline-1,3-dione, the title compound is prepared from 6-iodo-4-methoxymethylene-4H-isoquinoline-1,3-dione (85 mg, 0.26 mmol) and 5-Aminomethyl-2-butyl-phenol (54 mg, 0.3 mmol) in 65% yield: MS (ESI): 475.2 (M−1)−1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713994B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-0f895321f63846e8aeae3868fb82d545 |
| Source note | uspto-grants-2010_05 |