HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Aminomethyl)-4-iodophenol → HCID 178518375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Aminomethyl)-4-iodophenol | HCID 59300029 | — |
| Reactant | 4-methoxymethylene-6-iodo-4H-isoquinoline-1,3-dione | HCID 68691019 | — |
| Reactant | HCID 178518360 | HCID 178518360 | — |
| Product | HCID 178518375 | HCID 178518375 | 73% |
Reaction Steps
Following the same procedure for the preparation of 4-{[(2-Hydroxy-biphenyl-4-ylmethyl)-amino]-methylene}-6-iodo-4H-isoquinoline-1,3-dione, the title compound is prepared from 6-iodo-4-methoxymethylene-4H-isoquinoline-1,3-dione (100 mg, 0.30 mmol) and 3-Aminomethyl-4-iodo-phenol (80 mg, 0.32 mmol) in 73% yield: MS (ESI): 545.0 (M−1)−1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713994B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-8261fbc0ac9a4c42ac200b7d8a7c4b4f |
| Source note | uspto-grants-2010_05 |