HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Aminomethyl)-4-iodophenol → HCID 178518301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Aminomethyl)-4-iodophenol | HCID 59300029 | — |
| Reactant | 6-Furan-2-yl-4-methoxymethylene-4H-isoquinoline-1,3-dione | HCID 68696367 | — |
| Reactant | HCID 178518360 | HCID 178518360 | — |
| Product | HCID 178518301 | HCID 178518301 | 77% |
Reaction Steps
Following the same procedure for the preparation of 4-{[(2-Hydroxy-biphenyl-4-ylmethyl)-amino]-methylene}-6-iodo-4H-isoquinoline-1,3-dione, the title compound is prepared from 6-Furan-2-yl-4-methoxymethylene-4H-isoquinoline-1,3-dione (400 mg, 1.5 mmol) and 3-Aminomethyl-4-iodo-phenol (400 mg, 1.61 mmol) in 77% yield: MS (ESI): 485.1 (M−1)−1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713994B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-d1eb088139784bf8ad44c362d753e8ac |
| Source note | uspto-grants-2010_05 |