HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(Aminomethyl)-2-iodophenol → HCID 178518367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(Aminomethyl)-2-iodophenol | HCID 42625594 | — |
| Reactant | 6-Furan-2-yl-4-methoxymethylene-4H-isoquinoline-1,3-dione | HCID 68696367 | — |
| Reactant | HCID 178518360 | HCID 178518360 | — |
| Product | HCID 178518367 | HCID 178518367 | 80% |
Reaction Steps
Following the same procedure for the preparation of 4-{[(2-Hydroxy-biphenyl-4-ylmethyl)-amino]-methylene}-6-iodo-4H-isoquinoline-1,3-dione, the title compound is prepared from 6-Furan-2-yl-4-methoxymethylene-4H-isoquinoline-1,3-dione (60 mg, 0.22 mmol) and 5-Aminomethyl-2-iodo-phenol (58 mg, 0.23 mmol) in 80% yield: MS (ESI): 485.1 (M−1)−1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07713994B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-f521638052f14abe8dc2db0a18f03fb2 |
| Source note | uspto-grants-2010_05 |