HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2236887Generated: November 2, 2026
tert-Butoxy bis(dimethylamino)methane → HCID 74828433, compound
https://huagongshe.com/reaction/2236887
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | tert-Butoxy bis(dimethylamino)methane | HCID 79885 | — |
| Reactant | 1-(3-Furanyl)-4-methyl-2(1H)-pyridinone | HCID 42625744 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 74828433 | HCID 74828433 | — |
Reaction Steps
A mixture of 1-furan-3-yl-4-methyl-1H-pyridin-2-one (3.7 g, 21 mmol), tert-butoxybis(dimethylamino)methane (11 g, 63 mmol), and N,N-dimethylformamide (4 mL) is heated in a 150° C. oil bath for 2½ hours and then concentrated to dryness under reduced pressure. A quantitative yield of 4-(2-dimethylamino-vinyl)-1-furan-3-yl-1H-pyridin-2-one is assumed, and the material is carried on without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07713994B2 |
|---|
| Source dataset | uspto-grants-2010_05 |
|---|
| ORD ID | ord-aa02f9eba6284554836aa904a4ef6aa0 |
|---|
| Source note | uspto-grants-2010_05 |
|---|
