HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 70541530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 53688324 | HCID 53688324 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 70541530 | HCID 70541530 | — |
Reaction Steps
The title compound was prepared using the previously described procedure and the following reagants: t-butyl oxycarbonyl-methionyl-valyl-tryptophan (4.61 grams), 32 milliliters of glacial acetic acid and 17.5 ml (106.2 mmoles) 6.07 N hydrochloric acid in dioxane. Yield is 3.2 grams. Analysis calculated for C21H30N4O4S.HCL.H2O: C, 51.57; H, 6.80; N, 11.46. Found: C, 51.29; H, 6.59; N,-11.72.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04356118 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-3fe4852ccf014553b9591cea2df7e8d4 |
| Source note | uspto-grants-1982_10 |