Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 223694Generated: October 31, 2026

Acetic Acid → HCID 70542448, compound

https://huagongshe.com/reaction/223694

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantHydrochloric AcidHCID 313—
ReactantWaterHCID 962—
ReactantHCID 53933398HCID 53933398—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 70542448HCID 70542448—

Reaction Steps

The title compound is prepared using the previously described procedures and the following reagants: 1.17 g (2.3 mmoles) t-butyloxycarbonyl-isoleucyl-valyl-tryptophan, 10 ml glacial acetic acid and 10 ml 6.07 HCl in dioxane. Total yield was 0.91 g. (88 percent). Analysis calculated for C22H32N4O4.HCl. H2O: C, 56.10; H, 7.49, N, 11.90. Found: C, 56.34; H, 7.48; N, 11.72.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04356118
Source datasetuspto-grants-1982_10
ORD IDord-86b55e511d5e46388fc0da42439c617f
Source noteuspto-grants-1982_10