HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 70542448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 53933398 | HCID 53933398 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 70542448 | HCID 70542448 | — |
Reaction Steps
The title compound is prepared using the previously described procedures and the following reagants: 1.17 g (2.3 mmoles) t-butyloxycarbonyl-isoleucyl-valyl-tryptophan, 10 ml glacial acetic acid and 10 ml 6.07 HCl in dioxane. Total yield was 0.91 g. (88 percent). Analysis calculated for C22H32N4O4.HCl. H2O: C, 56.10; H, 7.49, N, 11.90. Found: C, 56.34; H, 7.48; N, 11.72.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04356118 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-86b55e511d5e46388fc0da42439c617f |
| Source note | uspto-grants-1982_10 |