HCID 86761111, compound → HCID 86761110, compound

Participants

Reaction Steps

A solution of 1-methyl-3-(4-nitro-phenoxy)-pyrrolidine•TFA (0.34 g, 1.0 mmol) in ethanol (10 mL) is hydrogenated for one hour at atmospheric pressure over 10% Pd/C. The mixture is filtered through a pad of diatomaceous earth and concentrated under reduced pressure to give 4-(1-methyl-pyrrolidin-3-yloxy)-phenylamine•TFA as a black solid.

Provenance & Evidence