HCID 20520585, compound → HCID 12940897, compound

HRID 223711Notes

Reaction equation

HRID 223711 reaction equation
Br[CH:2]([CH2:7][C:8]1[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][CH:9]=1)[CH2:3][C:4]([OH:6])=[O:5].[C:15]([O:18][C:19]1[CH:27]=[CH:26][C:22]([C:23]([NH2:25])=[S:24])=[CH:21][CH:20]=1)(=[O:17])[CH3:16]>CN(C)C=O>[Cl:14][C:11]1[CH:12]=[CH:13][C:8]([C:7]2[N:25]=[C:23]([C:22]3[CH:26]=[CH:27][C:19]([O:18][C:15](=[O:17])[CH3:16])=[CH:20][CH:21]=3)[S:24][C:2]=2[CH2:3][C:4]([OH:6])=[O:5])=[CH:9][CH:10]=1

Participants

4

Reactant 2

HCID 20520585HCID 20520585, compoundHCID 22471965HCID 22471965, compound

Product 1

HCID 12940897HCID 12940897, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

In a similar manner to Example 1(a), 3-Bromo-3-(4-chlorobenzyl)propionic acid and 4-acetoxy-thiobenzamide are reacted in dimethylformamide solvent to give the title compound.

Sources & evidence

ORD record
ord-2be44dd06bf4486bb73ed44a6997f863
Source dataset
uspto-grants-1982_10
Patent number
US04356185

Reaction notes

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