HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid methylene chloride → HCID 86619130, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Reactant | HCID 86619131 | HCID 86619131 | — |
| Product | HCID 86619130 | HCID 86619130 | — |
Reaction Steps
The (2S)—N-tert-butoxycarbonyl-3-tert-butyl-L-alanine methyl ester (529 mg, 2.04 mmol) is stirred at RT in TFA/dichloromethane 1:3 (3 ml), and the solution is concentrated on a rotary evaporator and dried under high vacuum. 540 mg (97% of theory) of product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07718611B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-31d57d1a62364e709a624f6c6dd597a3 |
| Source note | uspto-grants-2010_05 |