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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2237378Generated: October 31, 2026

Trifluoroacetic acid methylene chloride → HCID 86619130, compound

https://huagongshe.com/reaction/2237378

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acid methylene chlorideHCID 21863450—
ReactantHCID 86619131HCID 86619131—
ProductHCID 86619130HCID 86619130—

Reaction Steps

The (2S)—N-tert-butoxycarbonyl-3-tert-butyl-L-alanine methyl ester (529 mg, 2.04 mmol) is stirred at RT in TFA/dichloromethane 1:3 (3 ml), and the solution is concentrated on a rotary evaporator and dried under high vacuum. 540 mg (97% of theory) of product are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07718611B2
Source datasetuspto-grants-2010_05
ORD IDord-31d57d1a62364e709a624f6c6dd597a3
Source noteuspto-grants-2010_05