HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 68470337, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 59302561 | HCID 59302561 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 68470337 | HCID 68470337 | — |
Reaction Steps
The product of step c) (17 mg, 0.067 mmol) was dissolved in 1 mL 1:1 acetic acid:CHCl3 and treated with N-bromosuccinimide (12 mg, 0.068 mmol). After 30. minutes, the reaction solution was added dropwise to a solution of saturated sodium bicarbonate and extracted with ethyl acetate. The organic extracts were concentrated to give the subtitle compound, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07718647B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-b37710babdc64f49a6a32a626e04153c |
| Source note | uspto-grants-2010_05 |