Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 68473086 | HCID 68473086 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 46849908 | HCID 46849908 | — |
Reaction Steps
The product of step b) was treated with 2 mL each of EtOH and 40% aqueous KOH. After heating to 100° C. for 12 hours, the reaction was cooled, diluted with water, and extracted 2× into DCM. The title product was purified by preparative HPLC-MS. MS: ESI (positive): 224 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07718647B2 |
|---|
| Source dataset | uspto-grants-2010_05 |
|---|
| ORD ID | ord-cf910cc00eaf41ad868313189653cbf7 |
|---|
| Source note | uspto-grants-2010_05 |
|---|
