Trimethylsilyl iodide → HCID 46849913, compound

Participants

Reaction Steps

A solution of the product from step c) (14.4 mg, 0.044 mmol) in CH2Cl2 (220 μl) was treated with iodotrimethylsilane (19 μl, 0.13 mmol) at 60° C. for 12 hours. The reaction was quenched by the addition of MeOH and the solvent was evaporated. The residue was purified by preparative LC/MS providing 2.3 mg (18%) of the title compound. MS: ESI (positive): 256 (M+H).

Provenance & Evidence