HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59006385, compound → 3-Ethylpyridin-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59006385 | HCID 59006385 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Ethylpyridin-2-amine | HCID 11051636 | 83.9% |
Reaction Steps
130 mg of the 2-nitro-vinylpyridine [120-1] was dissolved in 5 mL of ethanol, 65 mg of 10% palladiumcarbon catalyst was added thereto, and stirred overnight at room temperature in a hydrogen atmosphere. The insolubles were filtered through celite, the filtrate was concentrated under reduced pressure, and 88.7 mg of 3-ethylpyridin-2-amine [120-2] was obtained as a yellow oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07718801B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-a5a9bf2141d04bada4568a212eaaf274 |
| Source note | uspto-grants-2010_05 |