Hydrochloric Acid → HCID 10932491, compound

HRID 2239204Notes

Reaction equation

HRID 2239204 reaction equation
[CH2:1]=[O:2].O[CH:4]1[CH:11]2[CH2:12][CH:7]3[CH2:8][CH:9]([CH2:13][CH:5]1[CH2:6]3)[CH2:10]2.[ClH:14]>>[Cl:14][CH2:1][O:2][CH:4]1[CH:11]2[CH2:12][CH:7]3[CH2:8][CH:9]([CH2:13][CH:5]1[CH2:6]3)[CH2:10]2

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 712FormaldehydeHCID 641492-Adamantanol2×

Product 1

HCID 10932491HCID 10932491, compound

Procedure

Paraformaldehyde was added to 2-hydroxyadamantane, and a hydrogen chloride gas was injected at 2.5 equivalent amounts per this 2-hydroxyadamantane. Then, the reaction was conducted at a temperature of 50° C. for 12 hours. After the completion of the reaction, the product was distillated under reduced pressure so as to obtain 2-adamantyl chloromethyl ether (compound 2) represented by the following chemical formula (59).

Workup

  1. customAfter the completion of the reaction

Sources & evidence

ORD record
ord-4e5c2b198e7a46519b3199088e4b4b0d
Source dataset
uspto-grants-2010_05
Patent number
US07723007B2

Reaction notes

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